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Analysis of rheological behaviour of titanium feedstocks formulated with a water-soluble binder system for powder injection moulding

机译:用水溶性粘合剂体系配制的粉末注射成型钛原料的流变行为分析

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摘要

Binder selection and formulation are critical in powder injection moulding. Binders play a key role in controlling the rheological properties of a feedstock and influence whether the resulting feedstock can be successfully injection moulded, debound and sintered without defects. A four-step process was used to mix hydride-dehydride titanium alloy (processed) powder (Ti-6Al-4 V) with a polyethylene glycol (PEG) based water soluble binder system. The rheological properties, including flow behaviour index, flow activation energy, fluidity and melt flow index of the homogeneous feedstock, were determined with a capillary rheometer. All feedstock formulations exhibited shear thinning flow behaviour. The optimum feedstock consisting of 60 vol.% powder content, 32 vol.% PEG, 6 vol.% polyvinyl butyryl and 2 vol.% stearic acid was suitable for titanium injection moulding.
机译:粘合剂的选择和配方对于粉末注射成型至关重要。粘合剂在控制原料的流变性中起着关键作用,并影响所得原料是否可以成功地注塑,脱脂和烧结而没有缺陷。使用四步过程将氢化物-脱水钛合金粉末(加工后的粉末)(Ti-6Al-4 V)与基于聚乙二醇(PEG)的水溶性粘合剂体系混合。用毛细管流变仪测定流变性质,包括均相原料的流动行为指数,流动活化能,流动性和熔体流动指数。所有原料配方均表现出剪切稀化流动特性。由60%(体积)的粉末含量,32%(体积)的PEG,6%(体积)的聚乙烯丁酰和2%(体积)的硬脂酸组成的最佳原料适用于钛注射成型。

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